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Metal nanoparticle formation by laser ablation in liquids by Ana Menéndez-Manjón Tartiere

Metal nanoparticle formation by laser ablation in liquids

by Ana Menéndez-Manjón Tartiere
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Book cover type: Paperback
  • ISBN13: 9783849119843
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Tredition Gmbh
  • Publisher Imprint: Tredition Gmbh
  • Publication Date:
  • Pages: 208
  • Original Price: GBP 12.99
  • Language: English
  • Edition: N/A
  • Item Weight: 254 grams
  • BISAC Subject(s): General

Die Synthese von Nanomaterialien ist heuzutage eines der am intensivsten erforschten Felder in der Wissenschaft. Nanopartikel als Pulver oder Kolloide sind von besonderem Interesse z.B. aufgrund der Applikation als hervorragende Katalysatoren, Sensoren oder Magnete. Unter den technisch relevanten Generierungsmethoden präsentiert der Laserabtrag in Flüssigkeiten den Vorteil einer hohen Flexibilität in Bezug auf die Materialvielfalt mit einem verhältnismä ig einfach handhabbaren Verfahren. Metall-, Metalloxid- oder Keramik-Nanopartikel in organischen oder anorganischen Medien wurden in weltweit verteilten Laboren erzeugt. Da es sich um eine relativ neue Technik handelt, sind die Entstehungsmechanismen und wichtigsten Einflussgrö en noch unklar und umstritten. Im Rahmen dieser Arbeit wurden der Bildungsmechanismus der Metall-Nanopartikel in Flüssigkeiten durch Laserabtrag in Flüssigkeiten mit dem Ziel einer optimalen Verfahrensvariante sowie die Prozesskontrolle zur Herstellung von Nanopartikeln untersucht. Nach einem Rückblick auf die physikalischen Eigenschaften der Ausbreitung und Fokussierung von ultrakurzen Laserpulsen in Flüssigkeiten und die Bedeutung der Laser-induzierten Fragmentierung wird der Einfluss der Repetitionsrate auf die resultierende Partikelgrö enverteilung analysiert und dargestellt. Die physikalischen Eigenschaften der Flüssigkeit infolge der Temperaturänderungen werden von der ersten Phase der Keimbildung in laserinduzierten Kavitationsblasen diskutiert. Anschlie end wird die Wachstumskinetik in der Flüssigkeit durch Koaleszenz von Plasmon-Spektroskopie bestimmt. Schlie lich wird die Anwendung des hochreinen und polydispersen Kolloides für die elektrophoretische Abscheidung gezeigt.

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