Allgemeine Untersuchungsmethoden: Zweiter Teil

Name: Allgemeine Untersuchungsmethoden: Zweiter Teil
Brand: Springer
SKU: 9783642855535
Price: 5148.0 INR
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by Heinz Bartels

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ISBN13: 9783642855535
Binding: Paperback
Subject: N/A
Publisher: Springer
Publisher Imprint: Springer
Publication Date: April 9, 2012
Pages: 1086
Original Price: EUR 70.08
Language: German
Edition: 10. Aufl. 1955.
Item Weight: 2432 grams
BISAC Subject(s): Research

About The Book

membran ist mechanisch wenig widerstandsfahig. Urn ihr den bei hohenDrucken unbe- dingt notigen Halt zu geben, wurde von diesen Autoren wiederum der Weg gewahlt, daB die Membran in den Poren einer Tonfilterkerze niedergeschlagen wurde. MORSE fand, daB eine Verbesserung der Membranen erzielt wird, wenn die Ionen durch elektrischen Transport in die Filterporen eingebracht werden. Zur Entfernung der Luft wurde die Zelle zuerst in verdiinnte Kaliumsulfatlosung gestellt und die Kathode innen, die Anode auBen angebracht, so daB durch elektrische Endosmose ein Wasserstrom entstand, der die Luft aus den Poren verdrangte. Danach wurde die Zelle sorgfaltig salzfrei gewaschen, mit Tetrakaliumhexacyanoferrat gefiillt und in Kupfersulfat gestellt. Von einer Kupferanode auBen ging der Strom zu einer Platinkathode innen. Dieser Vorgang wurde mehrmals unter jeweiliger Priifung des mit der Membran erreichbaren osmotischen Druckes wiederholt, bis dieser nicht weiter ge- steigert werden konnte. Wie sehr es auf technische Einzel- heiten ankommt, zeigt recht eindriicklich die Angabe von MORSE und FRAZER 1, daB von 500 vom Topfer gelieferten Zellen keine einzige taugliche Membranen ergab. Die notige Feinheit wurde nur erreicht, wenn die nasse Tonerde durch ein seidenes Siebtuch von etwa 2600 Lochern je Quadrat- zentimeter gepreBt und nachher unter dem Druck von 200 Tonnen wahrend 14-16 Std geformt wurde. MORSE und FRAZER verwendeten geschlossene Manometer, die mit Stickstoff . gefiillt waren und vorher kalibriert wurden. Mit ihren Apparaturen waren die Autoren imstande, Drucke bis zu 30 Atm. sehr genau zu messen.

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