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Anleitung Zur Quantitativen Bestimmung Der Organischen Atomgruppen by Hans Meyer

Anleitung Zur Quantitativen Bestimmung Der Organischen Atomgruppen

by Hans Meyer
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Book cover type: Paperback
  • ISBN13: 9783642901041
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Springer
  • Publisher Imprint: Springer
  • Publication Date:
  • Pages: 204
  • Original Price: EUR 51.39
  • Language: German
  • Edition: Softcover Repri
  • Item Weight: 259 grams
  • BISAC Subject(s): Chemistry / Organic

Auflage eine gleieh freundliche Anfnahme finden wird Wle ihre V orgiingerin. Dass aueh im Auslande Interesse fUr den behandelten Gegenstand vorhanden ist, beweist die Tatsaehe, dass die durch Herrn B. Tingle besorgte englische Ubersetzung meiner Anleitung bereits im Vorjahre in zweiter Auflage ersehienen ist. Herrn Dr. Otto Honigschmid danke ieh herzliehst fUr seine U nterstutzung beim Lesen der Korrekturen. Prag, im Januar 1904. Del' Verfasser. Illhaltsvel'zeiclmis. Seile Einleitung. . . . . . . 1 I. Bestimmung del' Hydroxylgruppe 3 A. Acetyliel'ungsmethoden . . . . . 5 1 Die Vel'fahren zur Acetylierung . 5 a) Acetylierung miUelst Acetylchlorid 5 b) Acet. ylierung mit Essigsiiureanhydl'id 7 cj Acetylierung durch Eisessig . . . 11 d) Acetylierung durch Uhloracetylchlorid 11 Nicht acetyliel'bare Hydroxyle 11 2. Iso lie rung del' Acetylprodllktl'. U 3. Bestimmung del' Acetylgruppeu 13 a) Verseifungsmethoden. . . 13 b) Additionsmethode . . . . 22 c) Wagung des Kaliumacetats 22 d) Destillationsverfahren 23 B. Benzoylielungsmethoden. . . . 24 1. Verfahl'en zur Benzoylierung . 24 a) Benzoylieren miitelst Bem: oylchlorid 25 b) Benzoylieren mit Benzoesiiureanhydrid 28 c) Benzoylieren mittelst substituiel'ter Benzoesaurederivate und A Karboxylgl'uppe durch Analyse del' Metall- salze del' Saul'e . . . . . . . . . . . . . . . . 45 J nhaltsverzeichnis. VIII Seite B. 'l'itration der Sliuren. 47 C. Indirekte Methoden . 49 1. Karbonatmethode .

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