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Chemische Laboratoriumstechnik: Ein Hilfsbuch Für Laboranten Und Fachschüler by Egbert V. Schivizhoffen, Walter Wittenberger

Chemische Laboratoriumstechnik: Ein Hilfsbuch Für Laboranten Und Fachschüler

by Egbert V. Schivizhoffen , Walter Wittenberger
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Book cover type: Paperback
  • ISBN13: 9783709175507
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Springer
  • Publisher Imprint: Springer
  • Publication Date:
  • Pages: 328
  • Original Price: EUR 74.76
  • Language: German
  • Edition: Softcover Repri
  • Item Weight: 413 grams
  • BISAC Subject(s): Chemistry / General

1. Unfallgefahren und Unfallschutz.- A. Umgang mit chemischen Stoffen.- B. Sicherheitseinrichtungen 3 Allgemeine Sicherheitsmaßnahmen.- C. Erste Hilfe bei Unfällen.- 2. Einrichtung des chemischen Laboratoriums.- A. Allgemeine Einrichtung.- B. Arbeitsgeräte.- C. Werkstoffe.- 3. Hilfsmittel beim Aufbau von Apparaturen.- A. Glasblasen.- B. Die Spritzflasche.- C. Reinigen der Laboratoriumsgeräte.- D. Behandeln von Kork, Gummi und Asbest.- E. Verbinden von Apparateteilen.- F. Verschiedenes.- 4. Zerkleinern, Sieben und Sichten.- A. Zerkleinern.- B. Sieben und Sichten.- 5. Mischen.- A. Rühren.- B. Schütteln.- C. Umlaufpumpen.- 6. Wägen.- A. Allgemeines.- B. Feinwaagen.- C. Präzisionswaagen.- D. Technische Waagen.- E. Besondere Maßnahmen beim Wägen.- F. Wägegefäße.- 7. Abmessen von Flüssigkeiten.- A. Allgemeines.- B. Tropfgefäße.- C. Meßzylinder und Meßkolben.- D. Pipetten und Büretten.- E. Dosieren von Flüssigkeiten.- F. Umfüllen von Flüssigkeiten.- 8. Lösen.- Allgemeines.- Arten der Lösung.- Lösungsmittel.- Herstellen einer Lösung.- 9. Trennung fest/flüssig.- A. Dekantieren.- B. Filtermaterial.- C. Filtrieren unter normalem Druck.- D. Filtrieren unter vermindertem Druck (Absaugen).- E. Filtrieren unter Druck.- F. Schleudern (Zentrifugieren).- G. Ultrafiltration. Dialyse.- 10. Hinweise für analytische Arbeiten.- Lösen fester Stoffe auf chemischem Wege.- Aufschließen unlöslicher Stoffe.- Auflösen erstarrter Schmelzen.- Fällen.- Filtrieren.- Auswaschen von Niederschlägen.- Trocknen, Veraschen und Glühen von Niederschlägen.- Abrauchen.- Tüpfelanalyse.- Schnelltest für die Bestimmung von Ionen.- Schäumen von Flüssigkeiten.- 11. Trocknen, Heizen und Kühlen.- A. Trocknen fester Stoffe.- B. Trocknen von Flüssigkeiten.- C. Direkte Heizung.- D.Heizbäder.- E. Thermostaten und Wärmetauscher.- F. Kühlen fester und flüssiger Stoffe.- G. Kühlen von Dämpfen.- 12. Temperaturmessung und -regelung.- A. Temperaturmessung.- B. Temperatur-Regulierung.- 13. Verdampfen, Destillieren und Sublimieren.- A. Verdampfen.- B. Einfache Destillation.- C. Fraktionierte Destillation.- D. Azeotrope Destillation.- E. Vakuumdestillation.- F. Sublimieren.- 14. Extrahieren und Verteilen (Ausschütteln).- A. Extrahieren.- B. Multiplikative Verteilung.- 15. Adsorbieren.- A. Adsorption.- B. Chromatographie.- 16. Kristallisieren.- A. Umkristallisieren.- B. Fraktionierte Kristallisation und Zonenschmelzverfahren.- 17 Charakteristische Temperaturen.- Schmelzpunkt.- Erstarrungspunkt.- Siedepunkt.- Universelle Apparate.- Flammpunkt.- 18. Dichte.- Allgemeines.- Pyknometer.- Auftriebsmethoden.- Aräometer.- Dichtemeßeinrichtung für Flüssigkeiten und Gase nach Kratky, Leopold und Stabinger.- Bestimmung der Gasdichte.- Schütt- und Rüttelgewicht.- 19. Viskosität.- Allgemeines.- Viskosimeter nach Ubbelohde.- Viskosimeter nach Höppler.- Rotationsviskosimeter.- Balance-Rheometer nach Dr. Képès.- 20. Arbeiten mit Gasen.- A. Gasbehälter.- B. Herstellen von Gasen im Laboratorium Gasentwicklungsapparate.- C. Reinigen und Trocknen von Gasen Wasch- und Trockenapparate.- D. Gasanalyse Gasanalytische Methoden.- E. Messen strömender Gase Volumetrische Gasmesser.- 21. Vakuum- und Drucktechnik.- A. Erzeugung von Vakuum.- C. Messen des Druckes.- D. Regeln des Druckes.- E. Rühren unter Luftabschluß.- 22. Probenahme.- Feste Stoffe.- Flüssigkeiten.- Gase.- 23. Elektroanalytische Verfahren.- A. Elektrolyse.- B. Elektrische Indikationsverfahren.- C. Polarographie.- D. Elektrophorese.- 24. pH-Messung.- Allgemeines.- Elektrometrische pH-Messung.-Colorimetrische pH-Messung.- 25. Optische Verfahren.- Mikroskop.- Polarimetrie.- Refraktometrie.- Interferometrie.- Colorimetrie.- Photometrie.- Absorptionsspektroskopie.- Emissionsspektralanalyse.- 26. Elementaranalyse.- Methoden.- Verbrennungsapparatur.- Benutzte und einschlägige Literatur.

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