Desenvolvimento de métodos para a amlodipina e a nevirapina por UVS e HPTLC

Name: Desenvolvimento de métodos para a amlodipina e a nevirapina por UVS e HPTLC
Brand: Edicoes Nosso Conhecimento
SKU: 9786630067477
Price: 7340.0 INR
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by Sathis Kumar Dinakaran , Narayudu Yandamuri

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ISBN13: 9786630067477
Binding: Paperback
Subject: N/A
Publisher: Edicoes Nosso Conhecimento
Publisher Imprint: Edicoes Nosso Conhecimento
Publication Date: May 24, 2026
Pages: 88
Original Price: GBP 58.0
Language: Portuguese
Edition: N/A
Item Weight: 127 grams
BISAC Subject(s): Pharmacology

About The Book

Foram desenvolvidos um m�todo simples, econ�mico e preciso de rela��o de absor��o por espectroscopia UV e um m�todo HPTLC para a determina��o simult�nea de besilato de amlodipina (AML) e nevirapina (NEV) em mat�ria-prima e na forma farmac�utica de comprimidos. Na espectroscopia, utilizou-se HCl 0,1 M como diluente para dissolver o AML e a NEV. As absor��es foram observadas a 252 nm (ponto isob�stico) e 295 nm (λmax da NEV), que foram selecionados com base na sobreposi��o dos espectros do AML e da NEV. Verificou-se que o intervalo de linearidade do m�todo UV era de 3-7 g/ml a 252 nm para a AML (r = 0,9995 0,0005) e a 295 nm para a NEV (r = 0,9985 0,0012). O m�todo HPTLC foi desenvolvido com placa de TLC de s�lica gel GF. Utilizou-se clorof�rmio-metanol-�cido ac�tico glacial (75,8:21,6:2,6) como diluente. A mancha ap�s o cromatograma foi identificada na c�mara UV e de iodo. Verificou-se que o intervalo de linearidade do m�todo HPTLC era de 5-25 g/ml para o AML (r = 0,9994) e de 295 nm para o NEV (r = 0,999). Foram realizados estudos de recupera��o dos m�todos UV e HPTLC para confirmar a precis�o dos m�todos. Os m�todos foram validados de acordo com as diretrizes da ICH. Verificou-se que os m�todos s�o simples, precisos, exatos e r�pidos para a determina��o simult�nea de AML e NEV em mat�ria-prima e na forma farmac�utica de comprimidos.

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