Die Chemische Untersuchung Des Eisens: Eine Zusammenstellung Der Bekanntesten Untersuchungsmethoden Für Eisen, Stahl, Roheisen, Eisenerz, Kalkstein, S
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Der Verfasser hat die Absicht, m dem vorliegenden Buche dem Eisenhüttenchemiker in möglichst kurz gefasster Form die verschiedenen Methoden der Eisen- und Stahl- u. s. w. Untersuchung, sowie die dazu nöthigen Apparate und Geräthschaften vorzuführen. Trotzdem ich mich nach Möglichkeit bemüht habe, das Original genau zu übersetzen, so sah ich mich doch, beson- ders im ersten Abschnitt, genöthigt, einige Aenderungen vor- zunehmen, da die vom Verfasser beschriebenen Apparate zum Theil veraltet, zum Theil auch für hiesige Verhältnisse nicht angebracht sind. Auch bei den Untersuchungsmethoden selbst habe ich mich bestrebt, den Verhältnissen auf deutschen Hüttenwerken Rechnung zu tragen, und ausseI' den vom Verfasser ange- führten noch einige andere Methoden hinzugefügt, wie sie auf hiesigen Werken eingeführt sind. l\Iülheim um Rhein, im März 1892. Der Uebel'setzer. Inhaltsverzeichniss. Seite Apparate . . . . . . . . 1 Apparate zur Bereitung der Proben 1 Allgemeine Laboratoriumsapparate . G Reagentien. . . . 23 Säuren und Salzbildner; Gase; Alkalien; Salze der Alkalien; Salze der alkalischen Erden; Metalle und Metallsalze; Reagentien zur Phosphorbestimmung. Methoden zur Untersuehung von Roheisen, Sehmiedeisen u. Stahl . 47 Bestimmung von Schwefel. . . . . . . . . . . - . . 47 Durch Entwicklung als H2S. Absorption durch eine alka- lische Lösung von salpetersaurem Blei. Durch eine ammoniakalische Lösung von schwefelsaurem Kadmium. Durch ammoniakalische Lösung von salpetersaurem Silber. Absorption und Oxydation vermittelst Brom und Salz- säure. Absorption und Oxydation durch übermangan- saures Kalium. Absorption und Oxydation durch Wasser- stoffsuperoxyd. Durch Oxydation und Lösung. Besondere Vorsichtsmaassregeln bei der Bestimmung von Schwefel in Roheisensorten. Schnell ausführbare Methoden: Volu- metrische Bestimmung vermittelst Jod. Viborgh's kolori- metrische Methode.
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