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Elektronenanlagerungs-Massenspektrographie Organischer Substanzen by Manfred V. Ardenne, K. Steinfelder, R. Tümmler

Elektronenanlagerungs-Massenspektrographie Organischer Substanzen

by Manfred V. Ardenne , K. Steinfelder , R. Tümmler
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Book cover type: Paperback
  • ISBN13: 9783540052876
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Springer
  • Publisher Imprint: Springer
  • Publication Date:
  • Pages: 404
  • Original Price: EUR 74.76
  • Language: German
  • Edition: N/A
  • Item Weight: 654 grams
  • BISAC Subject(s): Physics / General

Bei der Durchsicht der bisher vorliegenden umfangreichen Sammlungen von Massenspektren organischer Substanzen fällt auf, da es sich durchweg um Spektren pos i t i ver Ionen handelt und da keine Spektren ne g at i ver Ionen existieren. Betrachtet man die Zusammenhänge näher, so erkennt man, da die Ursache hierfür in erster Linie in der um einige Zehnerpo- tenzen geringeren Bildungswahrscheinlichkeit der negativen Ionen zu suchen ist. Die bekannten, relativ einfachen Verfahren zur Erzeugung positiver Ionen und die Stabilität der gebildeten Ionen sind weitere Faktoren, die dazu geführt haben, da praktisch nur positive Ionen zur massenspektrosko- pisehen Analyse verwendet wurden. Trotzdem erschien es aussichtsvoll, auch Massenspektren negativer Ionen, besonders für die Untersuchung or- ganischer Substanzen, heranzuziehen. Die unterschiedlichen Ionisierungs- mechanismen bei positiven und negativen Ionen lie en Unterschiede in den Massenspektren und damit zusätzliche Informationen über das Molekül und seinen Aufbau erwarten. Auf Grund der Tatsache, da die Auftrittspoten- tiale der negativen Ionen bei sehr niedrigen Werten liegen, war au erdem anzunehmen, da eine entsprechend geringe Energiezufuhr beim Ionisie- rungsvorgang zufragmentärmeren Spektren führt. Solche Spektren sind be- sonders bei Substanzen mit sehr schwachen Molekülpeaks und bei Substanz- gemischen von Vorteil. Zur Erzielung aussagekräftiger Massenspektren negativer Ionen fehlten je- doch zunächst die physikalisch-technischen Voraussetzungen.

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