Entwicklung von Nickeloxid-Dünnschichten für die Umweltgassensorik

Name: Entwicklung von Nickeloxid-Dünnschichten für die Umweltgassensorik
Brand: Verlag Unser Wissen
SKU: 9786630068368
Price: 5317.0 INR
Availability: InStock

by Ravishankar Ramesh Ambi

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ISBN13: 9786630068368
Binding: Paperback
Subject: N/A
Publisher: Verlag Unser Wissen
Publisher Imprint: Verlag Unser Wissen
Publication Date: May 31, 2026
Pages: 72
Original Price: GBP 42.0
Language: German
Edition: N/A
Item Weight: 109 grams
BISAC Subject(s): Physics / General

About The Book

Dieses Buch befasst sich mit der Synthese und Charakterisierung von NiO, das mit der Methode der chemischen Badabscheidung unter Verwendung einer L�sung von Ni(NO3)2.6H2O abgeschieden wurde. Die R�ntgenbeugungsuntersuchung zeigte eine kubische Kristallstruktur von NiO mit einer bevorzugten Ausrichtung entlang (200). Die rasterelektronenmikroskopischen Aufnahmen zeigten eine por�se Strukturmorphologie, die aus Nanobl�ttern besteht. Das Netzwerk aus miteinander verbundenen Nanobl�ttern und Hohlr�umen bietet eine gro e Anzahl von Wegen und reaktiveren Stellen f�r die Gasdiffusion. Das TEM-Bild zeigt eine durchschnittliche Gr� e von 5 nm f�r NiO. Das AFM zeigt eine Rauheit von 107,9 nm f�r das nach 7 Stunden abgeschiedene NiO. Die BET-Messung ergibt eine spezifische Oberfl�che von 110,42 m2g-1. Die XPS-Studie zeigte, dass auf der NiO-Oberfl�che gemischte chemische Ni2+- und Ni3+-Zust�nde von Ni bei etwa 853,70 bzw. 855,44 eV vorhanden sind, was auf die Nicht-St�chiometrie des Films zur�ckzuf�hren ist. Die direkte Bandl�ckenenergie von etwa 3,6-3,7 eV wurde durch UV-Vis-Messungen f�r alle NiO-Filme ermittelt. 45,6 % Reaktion auf 100 ppm NO2 bei 200 C mit T_response = 13 s und T_recovery = 146 s. Die h�chste Reaktion von 45,6 % auf 100 ppm NO2 zeigt, dass NiO ein guter Kandidat f�r die Umwelt�berwachung bei moderater Arbeitstemperatur von 200 C ist.

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