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Herstellung und Charakterisierung von Zn-substituierten Cu-Cr-Ferriten by Hina Nazli, Safia Anjum

Herstellung und Charakterisierung von Zn-substituierten Cu-Cr-Ferriten

by Hina Nazli , Safia Anjum
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Book cover type: Paperback
  • ISBN13: 9786209607042
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Verlag Unser Wissen
  • Publisher Imprint: Verlag Unser Wissen
  • Publication Date:
  • Pages: 60
  • Original Price: GBP 42.54
  • Language: German
  • Edition: N/A
  • Item Weight: 96 grams
  • BISAC Subject(s): Electronics / General

Dieses Forschungsprojekt zielt darauf ab, Zink-substituierte Kupfer-Chrom-Spinellferrite mit der Zusammensetzung ZnxCu1-x Cr0,5Fe1,5O4 (wobei x = 0, 0,2, 0,4, 0,6, 0,8) herzustellen und zu charakterisieren, die durch pulvermetallurgische Verfahren unter Verwendung von 99,99 % handels�blichem ZnO, CuO, Cr2O3 und Fe2O3 als Ausgangsmaterial hergestellt werden. Das genau abgewogene Pulver wurde in einer Kugelm�hle gemahlen und 24 Stunden lang bei 1100 C kalziniert. Anschlie end wurden die kalzinierten Pulver mit einem A-Gate-Motor-St� el homogenisiert und dann 10 Stunden lang bei 900 C gesintert. Die thermischen, strukturellen, morphologischen, elementaren, magnetischen, optischen und dielektrischen Eigenschaften wurden jeweils mit TGA-DTA, XRD, FESEM, EDS, VSM, FTIR und LCR-Messger�t untersucht. Die TGA-DTA-Daten liefern die optimale Temperatur f�r die Herstellung von Spinellferriten, und sp�tere XRD-Mikroskopaufnahmen zeigen die Bildung einer einphasigen Spinellstruktur mit zunehmenden Gitterparametern und abnehmender R�ntgen- und Sch�ttdichte bei steigendem Zn-Gehalt. FESEM zeigt das aggregierte Kornwachstum. FTIR-Spektren zeigen zwei markante Banden im Bereich von 400-800 cm-1, die die Bildung von Spinellferriten best�tigen. Die dielektrische Verlustfunktion und die Dielektrizit�tskonstante (ε) nehmen mit steigender Frequenz ab.

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