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Metallografische Präparation von Uran-Molybdän by Dodenhöft, Matthias

Metallografische Präparation von Uran-Molybdän

by Matthias Dodenhöft
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Book cover type: Paperback
  • ISBN13: 9783656951926
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Grin Verlag
  • Publisher Imprint: Grin Verlag
  • Publication Date:
  • Pages: 84
  • Original Price: USD 67.9
  • Language: German
  • Edition: N/A
  • Item Weight: 123 grams
  • BISAC Subject(s): Mechanics / Thermodynamics

Bachelorarbeit aus dem Jahr 2013 im Fachbereich Physik - Angewandte Physik, Note: 1,0, Technische Universität München (FRM 2), Veranstaltung: Bachelorarbeit, Sprache: Deutsch, Abstract: Im Rahmen der geplanten Umrüstung des FRMII auf einen Kernbrennstoff mit niedrigerem Anreicherungsgrad ist die metallographische Präparation der Legierung Uran-Molybdän für verschiedene materialwissenschaftliche Untersuchungen von gro er Bedeutung. Uran-Molybdän hat sich schon in der Vergangenheit als ein erfolgversprechender Kandidat für die Umrüstung von Forschungsreaktoren etabliert. Nur durch weitere Analysen kann überprüft werden, inwiefern diese Legierung auch als zukünftiger hochdichter Kernbrennstoff des FRM II geeignet ist. In Bezug auf die metallurgische Untersuchung der Gefügestruktur ist die korrekte Präparation von Uran-Molybdän ein zentrales Element. Informationen über eine geeignete Vorgehensweise bei der metallographischen Präparation dieser Legierung sind in der entsprechenden Fachliteratur bisher kaum vorhanden. Aus diesem Grund erfolgen im Rahmen dieser Arbeit systematische Untersuchungen, wobei für jeden Präparationsschritt ein entsprechendes Verfahren entwickelt und optimiert wird. Verschiedene Festkörperphasen besitzen unterschiedliche mechanische und chemische Eigenschaften, sodass für alle relevanten Phasenzusammensetzungen von Uran-Molybdän und zusätzlich für reines, metallisches alpha-Uran geeignete Präparationsverfahren entwickelt werden. Durch den Vergleich unterschiedlich präparierter und analysierter Proben wird die Ausbildung eines Scheingefüges ausgeschlossen. Mit den entwickelten Verfahren ist eine mechanische Präparation der Proben ohne Schädigungen wie Kratzern oder einer Kantenverrundung gewährleistet. Zusätzlich konnte die Kornstruktur von alpha-Uran und der Legierung Uran-Molybdän bei allen Phasenzusammensetzungen mit verschiedenen Präparationsverfahren aufgedeckt werden. Auch die Dendritenstruktur der inhomogen verteilten gamma-Phase konnte si

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