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NMR-Spektroskopie. Eine Versuchsdurchführung by Mejid, Sadik

NMR-Spektroskopie. Eine Versuchsdurchführung

by Sadik Mejid , Markus Fetzer
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Book cover type: Paperback
  • ISBN13: 9783668965133
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Grin Verlag
  • Publisher Imprint: Grin Verlag
  • Publication Date:
  • Pages: 28
  • Original Price: GBP 27.5
  • Language: German
  • Edition: 1. Auflage
  • Item Weight: 50 grams
  • BISAC Subject(s): Chemistry / Organic

Praktikumsbericht / -arbeit aus dem Jahr 2015 im Fachbereich Chemie - Organische Chemie, Note: 1,3, Universität zu Köln (Organische Chemie), Sprache: Deutsch, Abstract: Die NMR-Spektroskopie ist eine der leistungsfähigsten instrumentellen Analysenmethoden in der Chemie. Sie ist heute unverzichtbar bei der Aufklärung von Molekülstrukturen. Es können kleine Moleküle wie auch recht gro e - bis zu Proteinen - untersucht werden. Die Bedeutung der Methode ist daran erkennbar, dass für deren Erforschung und Weiterentwicklung viermal der Nobelpreis verliehen worden ist. Aufgabenstellung: (1) Die Aufnahme eines 1H-NMR-Spektrums eines unbekannten Lösungsmittelgemisches in Chloroform und deren Analyse. Dazu sollten die Signale der Spektren und ihre Integrale Verbindungen zugeordnet werden und somit das unbekannte Lösungsmittelgemisch aus einem Satz verschiedener Lösungsmittel identifiziert werden. (2) Die Aufnahme der FID-Signale (Free Induction Decay) der Probe bei unterschiedlichen Pulslängen. (3) Die Bestimmung der Zentrumsfrequenz des aufgenommen 1H-Spektrums und eines 13C-Spektrums durch die Auswertung eines Inversion-Recovery-Experiments

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