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Nouveaux Phosphates d'Elément Trivalent by Lesage-J

Nouveaux Phosphates d'Elément Trivalent

by Lesage-J
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Book cover type: Paperback
  • ISBN13: 9786131556487
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Omniscriptum
  • Publisher Imprint: Omniscriptum
  • Publication Date:
  • Pages: 328
  • Original Price: GBP 83.0
  • Language: French
  • Edition: N/A
  • Item Weight: 481 grams
  • BISAC Subject(s): Chemistry / Inorganic

Ce travail explore la richesse structurale des phosphates à charpentes mixtes, qui comportent des cavités ou des feuillets susceptibles d'accueillir des cations en insertion. Ces matériaux trouvent des applications dans de nombreux domaines, notamment en catalyse. Nous avons isolé dix neuf nouvelles phases, par synthèse hydrothermale à basse température et par synthèse à l'état solide à haute température. Les déterminations structurales ont été effectuées par diffraction des rayons X sur monocristaux, systématiquement couplées à des études en DRX sur poudre, en EDS, et parfois complétée par des investigations en diffraction et microscopie électronique, en spectroscopie infrarouge et par des analyses thermogravimétriques. Nous avons également caractérisé l'activité d'une de ces phases en réduction sélective des oxydes d'azote, par spectrométrie de masse et en IR in situ et operando. L'analyse de ces structures, dont deux sont originales, met en évidence les relations existantes entre le mode de synthèse utilisé, la composition chimique étudiée et la structure obtenue. Un classement de ces structures en fonction de leur degré d'ouverture est finalement proposé.

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