Rozwój cienkich warstw tlenku niklu do wykrywania gazów środowiskowych

Name: Rozwój cienkich warstw tlenku niklu do wykrywania gazów środowiskowych
Brand: Wydawnictwo Nasza Wiedza
SKU: 9786630078602
Price: 5317.0 INR
Availability: InStock

by Ravishankar Ramesh Ambi

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ISBN13: 9786630078602
Binding: Paperback
Subject: N/A
Publisher: Wydawnictwo Nasza Wiedza
Publisher Imprint: Wydawnictwo Nasza Wiedza
Publication Date: June 4, 2026
Pages: 72
Original Price: GBP 42.0
Language: Polish
Edition: N/A
Item Weight: 109 grams
BISAC Subject(s): Physics / General

About The Book

Niniejsza książka dotyczy syntezy i charakterystyki NiO osadzonego metodą kąpieli chemicznej przy użyciu roztworu Ni(NO3)2.6H2O. Badanie dyfrakcji rentgenowskiej wykazalo sześcienną strukturę krystaliczną NiO z preferowaną orientacją wzdluż (200). Obrazy skaningowej mikroskopii elektronowej wykazaly porowatą strukturę morfologiczną zlożoną z nanosheets. Siec polączonych nanosiatek i pustek oferuje dużą liczbę ścieżek i bardziej reaktywnych miejsc do dyfuzji gazu. Obraz TEM ujawnia średni rozmiar 5 nm dla NiO. AFM ujawnia chropowatośc 107,9 nm dla NiO osadzonego po 7 h. Pomiar BET daje powierzchnię wlaściwą 110,42 m2g-1. Badanie XPS wykazalo obecnośc mieszanych stan�w chemicznych Ni2+ i Ni3+ odpowiednio przy okolo 853,70 i 855,44 eV na powierzchni NiO ze względu na niestechiometrię warstwy. Bezpośrednia energia przerwy pasmowej wynosząca okolo 3,6-3,7 eV zostala uzyskana za pomocą pomiaru UV-Vis dla wszystkich warstw NiO. Uzyskano 45,6% odpowiedź na 100 ppm NO2 w temperaturze 200 C przy T_response = 13 s i T_recovery = 146 s. Najwyższa odpowiedź 45,6% na 100 ppm NO2 pokazala, że NiO jest dobrym kandydatem do monitorowania środowiska w umiarkowanej temperaturze roboczej 200 C.

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