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Sintesi del titanato: diversi metodi e diversi precursori by Da Silva Magalhães, Renata

Sintesi del titanato: diversi metodi e diversi precursori

by Renata Da Silva Magalhães , Silvio R. Teixeira , Elson Longo
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Book cover type: Paperback
  • ISBN13: 9786208633578
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Edizioni Sapienza
  • Publisher Imprint: Edizioni Sapienza
  • Publication Date:
  • Pages: 60
  • Original Price: GBP 30.0
  • Language: Italian
  • Edition: N/A
  • Item Weight: 96 grams
  • BISAC Subject(s): General

I titanati di bario (BT) e stronzio (ST) sono stati prodotti con due metodi diversi, la reazione allo stato solido (SSR), a temperature di 1150/1200 C, e l'idrotermia assistita da microonde (MAH), con diverse concentrazioni del mineralizzatore KOH (1, 3 e 6 mol/L). Il cloruro di bario/stronzio e il TiO2 in fase anatasio sono stati utilizzati come precursori nella preparazione con il metodo SSR. Per le sintesi effettuate con il metodo MAH, sono stati utilizzati gli stessi cloruri e un complesso di anatasio con perossido di idrogeno come precursore del titanio. In tutte le preparazioni sono stati ottenuti titanati, ma con risultati diversi in termini di cristallizzazione e morfologia delle particelle, che possono essere associati alle diverse concentrazioni di mineralizzante, al tipo di precursore di titanio utilizzato e all'impiego di diverse strategie di sintesi. I materiali ottenuti dai due processi sono stati caratterizzati mediante diffrattometria a raggi X (XRD), spettroscopia micro-romana (MR), spettroscopia infrarossa a trasformata di Fourier (FTIR), UV-Vis, microscopia elettronica a scansione (SEM) e, infine, sono state registrate le loro emissioni fotoluminescenti (FL).

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