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Synthèse d'un étalon interne pour le bicalutamide by Maryam Amra Jordaan

Synthèse d'un étalon interne pour le bicalutamide

by Maryam Amra Jordaan , Jan Van Der Westhuizen
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Book cover type: Paperback
  • ISBN13: 9786208908898
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Editions Notre Savoir
  • Publisher Imprint: Editions Notre Savoir
  • Publication Date:
  • Pages: 92
  • Original Price: GBP 48.63
  • Language: French
  • Edition: N/A
  • Item Weight: 137 grams
  • BISAC Subject(s): Chemistry / General

Le (R, S)-Bicalutamide [N-(4-cyano-3-trifluorom�thylph�nyl)-α-m�thyl-α-hydroxy-β-(4- fluoroph�nylsulfonyl)propanamide], vendu sous le nom de Casodex(R), est le principal antiandrog�ne actuellement utilis� pour traiter le cancer de la prostate. Il se lie aux r�cepteurs androg�nes et bloque la croissance du cancer. Ce travail vise � d�velopper des �talons internes pour la composante bioanalytique des essais cliniques qui doivent d�tecter le bicalutamide et ses d�riv�s. Un �talon interne est ajout� � l'�chantillon de liquide corporel (principalement du sang) au d�but de la pr�paration de l'�chantillon, � une concentration � peu pr�s identique � celle de l'analyte � quantifier. Un �talon interne id�al pr�sente une r�cup�ration d'extraction et un temps de r�tention similaires dans la CLHP. Pour la quantification par spectrom�trie de masse, il doit pr�senter une diff�rence d'au moins 3 unit�s de masse par rapport � l'analyte et une r�ponse d'ionisation similaire. L'�talon interne est utilis� pour calibrer le courant ionique total du m�tabolite.

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