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Wytwarzanie i charakterystyka ferrytów Cu-Cr z domieszką cynku by Hina Nazli, Safia Anjum

Wytwarzanie i charakterystyka ferrytów Cu-Cr z domieszką cynku

by Hina Nazli , Safia Anjum
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Book cover type: Paperback
  • ISBN13: 9786209699207
  • Binding: Paperback
  • Subject: N/A
  • Publisher: Wydawnictwo Nasza Wiedza
  • Publisher Imprint: Wydawnictwo Nasza Wiedza
  • Publication Date:
  • Pages: 60
  • Original Price: GBP 38.19
  • Language: Polish
  • Edition: N/A
  • Item Weight: 96 grams
  • BISAC Subject(s): Electronics / General

Celem niniejszego projektu badawczego jest wytworzenie i scharakteryzowanie ferryt�w spinelowych miedziowo-chromowych z domieszką cynku o skladzie ZnxCu1-x Cr0,5Fe1,5O4 (gdzie x=0, 0,2, 0,4, 0,6, 0,8) przygotowanych metodami metalurgii proszkowej z wykorzystaniem dostępnych w handlu 99,99% ZnO, CuO, Cr2O3 i Fe2O3 jako materialu wyjściowego. Dokladnie odważony proszek zostal zmielony w mlynie kulowym i kalcynowany przez 24 godziny w temperaturze 1100 C. Następnie kalcynowane proszki zostaly zhomogenizowane przy użyciu tluczka z silnikiem A-gate, a następnie spiekane w temperaturze 900oC przez 10 godzin. Wlaściwości termiczne, strukturalne, morfologiczne, elementarne, magnetyczne, optyczne i dielektryczne zostaly zbadane odpowiednio przy użyciu TGA-DTA, XRD, FESEM, EDS, VSM, FTIR i miernika LCR. Dane TGA-DTA dostarczają optymalnej temperatury do wytwarzania ferryt�w spinelowych, a p�źniejsze mikrografy XRD ujawniają tworzenie się jednofazowej struktury spinelowej, wykazującej wzrost parametr�w sieci krystalicznej oraz spadek gęstości rentgenowskiej i objętościowej wraz ze wzrostem zawartości Zn. FESEM pokazuje agregowany wzrost ziarna. Widma FTIR wykazują dwa wyraźne pasma w zakresie 400-800 cm-1, co potwierdza tworzenie się ferryt�w spinelowych. Tangencja strat dielektrycznych i stala dielektryczna (ε) maleją wraz ze wzrostem częstotliwości.

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